Estimation of pH Essay Example for Free

Estimation of pH Essay Acid-base titration calculations Aim: This experiment is designed to train our skills of calculation in titration as well as help us to be familiar with the procedures of titration. Background: 1. Titration is a technique which involves measuring the volume of one solution which just reacts completely with another solution. 2. A pipette is designed to deliver exactly the same volume each time it is used. 3. A burette is equipment fitted with a tap and is calibrated so as to accurately measure a variable volume of solution. 4. Tire is the volume of the second solution required in titration. Method: The whole experiment is based on computer simulation. To train our calculation skills in titration, two trials are set. One is titration between a strong acid and a strong base. The other is between a weak acid and a strong base. In this experiment, the strong acid is HCl, the strong base is NaOH and the weak acid is CH3COOH. Strong acid and strong base 1. Set up the apparatus. 2. Measure 25ml Ba(OH)2 by pipette. 3. Transfer the Ba(OH)2 into a beaker. 4. Add Bromothymol Blue which is and indicator. 5. Add HCl into the burette. 6. Turn on the pH meter. 7. Insert the probes into the beaker. 8. Read the reading on burette. 9. Start titrating. 10. Read the final volume. 11. Remove the probes. Weak acid and strong base 1. Set up the apparatus. 2. Measure 25ml Ba(OH)2 by pipette. 3. Transfer the Ba(OH)2 into a beaker. 4. Add Bromothymol Blue which is and indicator. 5. Add CH3COOHhe burette. 6. Turn on the pH meter. 7. Insert the probes into the beaker. 8. Read the reading on burette. 9. Start titrating. 10. Read the final volume. 11. Remove the probes. Apparatus: Pipette 25ml Burette 50ml pH meter Beaker 80ml Chemicals: Barium Hydroxide, Ba(OH)2 Hydrochloric Acid, HCl Ethanoic Acid, CH3COOH Bromothymol Blue Safety: Follow the rules in the laboratory and wear the safety goggles. Set up of apparatus: Procedure: Strong acid and strong base 1. I set up the apparatus. 2. I measured 25ml Ba(OH)2 by pipette. 3. I transferred the Ba(OH)2 into a beaker. 4. I added Bromothymol Blue which is and indicator. 5. I added HCl into the burette. 6. I turned on the pH meter. 7. I inserted the probes into the beaker. 8. I read the reading on burette. 9. I started titrating. 10. I read the final volume. 11. I removed the probes. Weak acid and strong base 1. Set up the apparatus. 2. Measure 25ml Ba(OH)2 by pipette. 3. Transfer the Ba(OH)2 into a beaker. 4. Add Bromothymol Blue which is and indicator. 5. Add CH3COOHhe burette. 6. Turn on the pH meter. 7. Insert the probes into the beaker. 8. Read the reading on burette. 9. Start titrating. 10. Read the final volume. 11. Remove the probes. Data collection: Strong acid and strong base Initial pH in the beaker 15.03 Final pH in the beaker 2.79 Volume of HCl added 41.02ml Weak acid and strong base Initial pH in the beaker 14.90 Final pH in the beaker 2.57 Volume of HCl added 38.60ml Data processing: Strong acid and strong base The chemical equation for this reaction 2HCl(aq) + Ba(OH)2(aq) BaCl2(aq) + 2H2O(l) Weak acid and strong base The chemical equation for this reaction 2 CH3COOH (aq) + Ba(OH)2(aq) (CH3COOH)2Ba (aq) + 2H2O(l) Graph: Strong acid and strong base Screenshot of the software Graph of the pH in the beaker against volume added Weak acid and strong base Screenshot of the software Graph of the pH in the beaker against volume added Conclusion: The concentration of hydrochloric acid in the first trial is The concentration of ethanoic acid in the second trial is Evaluation and improvement: 1. As what I have discovered, all the graphs of a certain reaction in this software are the same. There is no difference in the graph if the concentration is changed. Also the graph is distinct points rather than a curve. During the experiment, sometimes failure occurred. Thus the only improvement could be done is to change another software.